Benzenesulfonyl isocyanate, 2-chloro- → HCID 23332187, 화합물

HRID 224213노트

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HRID 224213 반응식
[NH2:1][C:2]1[N:7]=[C:6]([O:8][CH3:9])[N:5]=[C:4]([NH:10][CH3:11])[N:3]=1.[Cl:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[S:19]([N:22]=[C:23]=[O:24])(=[O:21])=[O:20]>C(#N)C>[Cl:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[S:19]([NH:22][C:23]([NH:1][C:2]1[N:7]=[C:6]([O:8][CH3:9])[N:5]=[C:4]([NH:10][CH3:11])[N:3]=1)=[O:24])(=[O:21])=[O:20]

참가 물질

4

반응물 2

HCID 174071Benzenesulfonyl isocyanate, 2-chloro-HCID 233321882-Methoxy-4-amino-6-methylamino-1,3,5-triazine

생성물 1

HCID 23332187HCID 23332187, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매2회

실험 절차

To a solution of 2.1 g of 2-amino-4-methoxy-6-methylamino-1,3,5-triazine in 60 ml of hot acetonitrile was added, dropwise, 3.3 g of 2-chlorobenzenesulfonylisocyanate in 20 ml of acetonitrile. After stirring for 18 hours at room temperature, the mixture was filtered to yield the product named above melting at 224°-228°.

후처리

  1. filtrationthe mixture was filtered
  2. customto yield the product

출처 및 근거

ORD 기록
ord-9f3ba99375e04888bb514954a8a26cff
출처 데이터셋
uspto-grants-1980_11
특허 번호
US04231784

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