Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3,4-Dimethoxyphenyl)acetic acid → (3,4-Dimethoxyphenyl)acetyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3,4-Dimethoxyphenyl)acetic acid | HCID 7139 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | (3,4-Dimethoxyphenyl)acetyl chloride | HCID 3604458 | — |
반응 단계
3,4-Dimethoxyphenylacetic acid (6.47 g, 0.033 mole) was dissolved in 50 ml of dry benzene and refluxed for 2 hr. with excess thionyl chloride (25 ml). The solvent and SOCl2 were removed on a rotary evaporator. Two additional quantities of dry benzene were added to the residue, followed by rotary evaporation which yielded 3,4-dimethoxyphenylacetyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04232014 |
| 출처 데이터셋 | uspto-grants-1980_11 |
| ORD ID | ord-443b7a78d92843cb864c7a958b3edf6d |
| 출처 메모 | uspto-grants-1980_11 |