tert-Butyl (3-aminopropyl)carbamate → N,N'-bis(N-tert.butoxycarbonyl-3-amino propyl)-4-(6-phenylhexyloxy)-1,3-benzenedimethanamine
반응식
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]2[CH:19]=[CH:18][C:17]([CH:20]=O)=[CH:16][C:15]=2[CH:22]=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:24]([O:28][C:29]([NH:31][CH2:32][CH2:33][CH2:34][NH2:35])=[O:30])([CH3:27])([CH3:26])[CH3:25]>>[C:24]([O:28][C:29]([NH:31][CH2:32][CH2:33][CH2:34][NH:35][CH2:20][C:17]1[CH:18]=[CH:19][C:14]([O:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)=[C:15]([CH2:22][NH:35][CH2:34][CH2:33][CH2:32][NH:31][C:29]([O:28][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:30])[CH:16]=1)=[O:30])([CH3:27])([CH3:26])[CH3:25]참가 물질
3
실험 절차
N,N'-bis(N-tert.butoxycarbonyl-3-amino propyl)-4-(6-phenylhexyloxy)-1,3-benzenedimethanamine (MS: M+H+ =627) was prepared from 4-(6-phenylhexyloxy)-1,3-benzenedicarboxaldehyde and N-tert.butoxycarbonyl-3-aminopropanamine using the method in Example 2.
출처 및 근거
- ORD 기록
- ord-39c5a7b079d24a1c9553389079aa5a76
- 출처 데이터셋
- uspto-grants-1995_06