참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,6-Dimethoxybenzoic Acid | HCID 15109 | — |
| 반응물 | Sulfuryl chloride | HCID 24648 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 3-Chloro-2,6-dimethoxybenzoic acid | HCID 612199 | — |
반응 단계
A solution of 16.2 ml (0.2 mol) of sulphuryl chloride in 100 ml of chloroform is added dropwise while stirring to a solution of 36.4 g (0.2 mol) of 2,6-dimethoxybenzoic acid in 300 ml of chloroform. The mixture is heated for 0.5 h at 50° C. and left overnight at room temperature. The solvent is evaporated and the residue recrystallized from isopropyl ether--light petroleum. Yield: 35.4 g, m.p. 132°-33° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04232037 |
|---|
| 출처 데이터셋 | uspto-grants-1980_11 |
|---|
| ORD ID | ord-71ed333a1fb041258c5bd0fea60222fc |
|---|
| 출처 메모 | uspto-grants-1980_11 |
|---|
