Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thymol → HCID 23333158, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thymol | HCID 6989 | — |
| 반응물 | HCID 12878338 | HCID 12878338 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | HCID 23333158 | HCID 23333158 | — |
반응 단계
830 mg of 2,3-Dihydro-5-methyl-6-phenyl-benzofuran and 100 mg of palladium on charcoal are refluxed for 48 hours in 10 ml of freshly distilled p-cymol. After cooling, the mixture is filtered through talc and the filtrate evaporated. The residue is chromatographed on 15 g of Kieselgel. 5-Methyl-6-phenyl-benzofuran is eluted with toluene as a uniformly oily liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04232039 |
| 출처 데이터셋 | uspto-grants-1980_11 |
| ORD ID | ord-67a355f8859546deb5ea877ee89ccfc2 |
| 출처 메모 | uspto-grants-1980_11 |