참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Trimethylsilylacetylene | HCID 66111 | — |
| 반응물 | 3-Nitrophenyl azide | HCID 150927 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-(3-Nitro-phenyl)-4-trimethylsilanyl-1H-[1,2,3]triazole | HCID 68407374 | — |
반응 단계
Azido-3-nitro-benzene (CAS:1516-59-2, 11.8 g, 72 mmol) were dissolved in 20 ml THF and 30 ml trimethylsilylacetylene. The reaction mixture was stirred at 60° C. for 3 days. The solvents were evaporated off and the title compound was obtained as a brown solid (16.9 g, 90%), mp 75-78° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07678815B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_03 |
|---|
| ORD ID | ord-46412073a08d4be1babbe636a3492f41 |
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| 출처 메모 | uspto-grants-2010_03 |
|---|
