Benzene → 2,3-Dimethyl-5-allyl-6-tetradecanoylhydroquinone

HRID 224469노트

반응식

HRID 224469 반응식
C([O:4][C:5]1[C:10]([C:11](=[O:25])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])=[CH:9][C:8]([OH:26])=[C:7]([CH3:27])[C:6]=1[CH3:28])C=C.[CH:29]1[CH:34]=CC=C[CH:30]=1>>[CH3:28][C:6]1[C:7]([CH3:27])=[C:8]([OH:26])[C:9]([CH2:34][CH:29]=[CH2:30])=[C:10]([C:11](=[O:25])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[C:5]=1[OH:4]

참가 물질

3

반응물 2

HCID 241BenzeneHCID 233332484-Hydroxy-2,3-dimethyl-6-tetradecanoylphenyl allyl ether

생성물 1

HCID 205104582,3-Dimethyl-5-allyl-6-tetradecanoylhydroquinone

실험 절차

90 g of the allyl ether of step 2 were heated to 210° C. under nitrogen atmosphere within 2 h. After cooling the melt was dissolved in 300 ml of benzine (boiling range: 50°-75° C.) and placed in a cool place. The precipitate formed was filtered with suction the next day.

후처리

  1. temperatureAfter cooling the melt
  2. customThe precipitate formed
  3. filtrationwas filtered with suction the next day

출처 및 근거

ORD 기록
ord-7c05fbbb7b284f8d945e48ff232f998e
출처 데이터셋
uspto-grants-1980_11
특허 번호
US04232107

반응 노트

불러오는 중…