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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Acrylic Acid → Ammonium acrylate acrylic acid

HRID 2245600
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HRID 2245600 반응식
[C:1]([O-:5])(=[O:4])[CH:2]=[CH2:3].[NH4+:6].[C:7]([OH:11])(=[O:10])[CH:8]=[CH2:9]>O>[C:1]([O-:5])(=[O:4])[CH:2]=[CH2:3].[NH4+:6].[C:7]([OH:11])(=[O:10])[CH:8]=[CH2:9]
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참가 물질

4

반응물 2

HCID 6581Acrylic AcidHCID 161596Ammonium acrylate

생성물 1

HCID 19048366Ammonium acrylate acrylic acid

시약·촉매·용매 1

HCID 962Water용매

실험 절차

To a 300 ml separable flask, were added 171.13 g of a 40% by weight aqueous ammonium acrylate solution from Production Example 1, 18.53 g of acrylic acid, and 35.34 g of water to obtain a 38% by weight aqueous ammonium acrylate/acrylic acid=75/25 solution, which was then mixed with 7.8 g of activated carbon and stirred for one hour while shielding the light. The resulting solution was filtered to remove the activated carbon, followed by adding and dissolving 0.0968 g of trimethylolpropane triacrylate as a crosslinking agent. To a 300 ml separable flask, was transferred 90 g of the solution, which was then purged with nitrogen at 30° C. for 30 minutes under stirring. To the resulting solution, was added 0.018 g of sodium hydrogen sulfite and then 0.0276 g ammonium persulfate. Polymerization was performed for one hour to obtain a polymer, which was then crushed to about 5 mm and dried at 150° C. for one hour in an inert oven with a nitrogen atmosphere. The dried polymer was milled by a homogenizer and then classified into particles having a particle size of 106 to 850 μm. The classified polymer in an amount of 100 parts was mixed with 2 parts of propylene glycol, 3 parts of water, and 30 parts of isopropyl alcohol, followed by heat treatment at 150° C. for 60 minutes. The resin obtained as described above was named as a comparative water-absorbing resin (1).

출처 및 근거

ORD 기록
ord-93040412aea44a98b4618d31dcbafc71
출처 데이터셋
uspto-grants-2010_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07683150B2

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