참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydroxylamine | HCID 787 | — |
| 반응물 | N-(3-chloro-4-cyanophenyl)methanesulfonamide | HCID 669685 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Chloro-N'-hydroxy-4-[(methylsulfonyl)amino]benzenecarboximidamide | HCID 72533799 | — |
반응 단계
To a stirred solution of the product from Step A (0.13 g, 0.565 mmol) in ethanol (3 mL) was added hydroxylamine (50% in water, 1.0 mL). The reaction was heated at 90° C. for 2 h. The reaction was then concentrated to give the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07687492B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_03 |
|---|
| ORD ID | ord-29c660b8b31b4cfb89eb3c7c518f418c |
|---|
| 출처 메모 | uspto-grants-2010_03 |
|---|
