2-Methyl-4-amino-5-aminomethylpyrimidine carbonate → 4-Amino-2-methyl-5-pyrimidinemethanamine
반응식
C(=O)(O)O.[CH3:5][C:6]1[N:11]=[C:10]([NH2:12])[C:9]([CH2:13][NH2:14])=[CH:8][N:7]=1>C(O)(C)C>[CH3:5][C:6]1[N:11]=[C:10]([NH2:12])[C:9]([CH2:13][NH2:14])=[CH:8][N:7]=1참가 물질
3
반응 조건
- 온도
- 85 °C
실험 절차
An amount of 170 g of isopropanol was added to 30.0 g of the 2-methyl-4-amino-5-aminomethylpyrimidine carbonate thus obtained, followed by heating at about 85° C. for 180 minutes to give 2-methyl-4-amino-5-aminomethylpyrimidine with purity of 99.0%.
후처리
- customthus obtained
출처 및 근거
- ORD 기록
- ord-a50f703487d34e34a96e06a641c77b92
- 출처 데이터셋
- uspto-grants-1991_08
- 특허 번호
- US05037982
반응 노트
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