HCID 15591815, 화합물 → HCID 12763795, 화합물

반응식

Cl.[NH2:2][C:3]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:6]=[C:5]([CH3:14])[CH:4]=1.[C:15]([N:18]1[CH2:22][CH2:21][N:20]=[CH:19]1)(=[O:17])[CH3:16]>>[C:15]([N:18]1[CH2:22][CH2:21][N:20]=[C:19]1[NH:2][C:3]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:6]=[C:5]([CH3:14])[CH:4]=1)(=[O:17])[CH3:16]

참가 물질

반응물 2

HCID 15591815HCID 15591815, 화합물

HCID 202977753-methyl-1-phenyl-1H-pyrazol-5-amine hydrochloride

생성물 1

HCID 12763795HCID 12763795, 화합물

실험 절차

5-Amino-3-methyl-1-phenyl pyrazole hydrochloride (37.8 g.) and -1-acetyl-2-imidazoline (27.4 g.) were reacted as described in Example I to give 35.4 g. product. mp 153°-162° (crystallized from CH3CN)

후처리

customto give 35.4 g
custommp 153°-162° (crystallized from CH3CN)

출처 및 근거

ORD 기록: ord-b5a9b93bdfce451e9cf43afe91fcc5f7
출처 데이터셋: uspto-grants-1980_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04234594

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