Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Amino-4-chlorobenzoic acid → 3-[5-(1-t-Butoxyformamido)valeramido]-4-chlorobenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Amino-4-chlorobenzoic acid | HCID 76092 | — |
| 반응물 | 5-(((Tert-butoxy)carbonyl)amino)pentanoic acid | HCID 545848 | — |
| 생성물 | 3-[5-(1-t-Butoxyformamido)valeramido]-4-chlorobenzoic acid | HCID 53751622 | — |
반응 단계
For the preparation of the starting material, 5-[1-(t-butoxy)formamido]valeric acid and 3-amino-4-chlorobenzoic acid are coupled to give 3-[5-(1-t-butoxyformamido)valeramido]-4-chlorobenzoic acid, m.p. 203° C., and the latter is coupled with β-alanine t-butyl ester to give N-[3-[5-(1-t-butoxyformamido)valeramido]-4-chlorobenzoyl]-β-alanine t-butyl ester, MS: 498 (60, M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05039805 |
| 출처 데이터셋 | uspto-grants-1991_08 |
| ORD ID | ord-64055d80423c4760b5e2dd3b8fc9038a |
| 출처 메모 | uspto-grants-1991_08 |