Oxalyl chloride → HCID 14580088, 화합물

HRID 2248918노트

반응식

HRID 2248918 반응식
[C:1]([O:4][C:5]1[C:6]([CH3:20])=[C:7]([CH3:19])[C:8]2[O:12][CH:11]([CH2:13][C:14](O)=[O:15])[CH2:10][C:9]=2[C:17]=1[CH3:18])(=[O:3])[CH3:2].C(Cl)(=O)C([Cl:24])=O>C1C=CC=CC=1>[C:1]([O:4][C:5]1[C:6]([CH3:20])=[C:7]([CH3:19])[C:8]2[O:12][CH:11]([CH2:13][C:14]([Cl:24])=[O:15])[CH2:10][C:9]=2[C:17]=1[CH3:18])(=[O:3])[CH3:2]

참가 물질

4

반응물 2

HCID 65578Oxalyl chlorideHCID 65961Raxofelast

생성물 1

HCID 14580088HCID 14580088, 화합물

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

To a suspension of (RS)-2-(2,3-dihydro-5-acetyloxy-4,6,7-trimethylbenzofuranyl) acetic acid (see example 2) (4.4 g) in benzene (36 ml) is added dropwise oxalyl chloride (7 ml) over 30'.

출처 및 근거

ORD 기록
ord-26b644a7d41b4ca69d88408640a2b523
출처 데이터셋
uspto-grants-1991_08
특허 번호
US05041568

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