Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Urea → Urea, N-dodecyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Urea | HCID 1176 | — |
| 반응물 | Dodecylamine | HCID 13583 | — |
| 생성물 | Urea, N-dodecyl- | HCID 75091 | — |
반응 단계
250 g of urea were continuously introduced into a decomposer in the course of 2 hours. The pyrolysis gases were introduced into a melt of 1200 g of dodecylamine at a temperature of 80 to 90° C. After completion of the reaction, the excess dodecylamine was distilled off in vacuo and the residue was recrystallized from chloroform. 598.9 g, i.e. 63% of theory, of dodecylurea having a melting point of 105 to 107° C were obtained in this way.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05043444 |
| 출처 데이터셋 | uspto-grants-1991_08 |
| ORD ID | ord-ba76054d729446f582550ed1f8a40480 |
| 출처 메모 | uspto-grants-1991_08 |