Methanol → 70288-74-3

HRID 224956노트

반응식

HRID 224956 반응식
[CH3:1][O:2][C:3](=[O:7])[CH:4](Br)[CH3:5].[O-:8][C:9]#[N:10].[K+].[CH3:12][OH:13]>>[CH3:1][O:2][C:3](=[O:7])[CH:4]([NH:10][C:9]([O:13][CH3:12])=[O:8])[CH3:5]

참가 물질

4

반응물 3

HCID 887MethanolHCID 95576Methyl 2-bromopropionateHCID 11378442Potassium cyanate

생성물 1

HCID 642186470288-74-3수율 59%

실험 절차

From the reaction of 11.69 grams of 2-bromopropionic acid methyl ester with 8.52 grams of potassium cyanate and 7.85 grams of methanol under the conditions described in Example 1 there were isolated 6.66 grams (59%) of 2-methoxycarbonylaminopropionic acid methyl ester with a boiling point of 65°-67° C./0.0013 mbar.

출처 및 근거

ORD 기록
ord-17b1c62716884293a7f30fb49e02d387
출처 데이터셋
uspto-grants-1980_11
특허 번호
US04234744

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