Myristic Acid → Tetradecanoic acid, strontium salt (2:1)

HRID 225034

반응식

HRID 225034 반응식
[C:1]([OH:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].O.O.O.O.O.O.O.O.[OH-].[Sr+2:26].[OH-]>O>[C:1]([O-:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Sr+2:26].[C:1]([O-:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

참가 물질

4

반응물 2

HCID 11005Myristic AcidHCID 21617461Strontium hydroxide octahydrate

생성물 1

HCID 167169Tetradecanoic acid, strontium salt (2:1)

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
50 °C

실험 절차

100 of myristic acid which has been granulated from an aqueous emulsion as described in Example 1 (AN 246, titer 53° C. particle size 0.2-0.3 mm.) and 60.2 g strontium hydroxide octahydrate (97% active) are suspended in one liter of water at 50° C. temperature and stirred for 30 minutes at 50° C. followed by 60 minutes of agitation at 70° C. The hollow formed granulate is filtered and dried. The content of free fatty acid amounts to 1.7%.

후처리

  1. customtiter 53° C.
  2. waitfollowed by 60 minutes of agitation at 70° C
  3. filtrationThe hollow formed granulate is filtered
  4. customdried

출처 및 근거

ORD 기록
ord-0e0c9f328fc14207a0f5b0bbce5340c2
출처 데이터셋
uspto-grants-1980_11
특허 번호
US04235794

연결된 노트

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