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Sodium Methoxide → (5-Methoxy-biphenyl-3-yl)-thiourea

HRID 2250788
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인쇄 미리보기

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HRID 2250788 반응식
C([NH:9][C:10]([NH:12][C:13]1[CH:14]=[C:15]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[CH:16]=[C:17]([O:19][CH3:20])[CH:18]=1)=[S:11])(=O)C1C=CC=CC=1.C[O-].[Na+]>CO>[CH3:20][O:19][C:17]1[CH:18]=[C:13]([NH:12][C:10]([NH2:9])=[S:11])[CH:14]=[C:15]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[CH:16]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 10942334Sodium MethoxideHCID 222833191-Benzoyl-3-(5-methoxy-biphenyl-3-yl)-thiourea

생성물 1

HCID 22283392(5-Methoxy-biphenyl-3-yl)-thiourea수율 88%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

1-Benzoyl-3-(5-methoxy-biphenyl-3-yl)-thiourea (183 mg, 0.51 mmol) in methanol (5 ml) are treated with sodium methoxide (5.4M in methanol, 0.14 ml) and the formed precipitate is filtered off. Washing with methanol yields the product (115 mg, 88%) as off-white powder. MS: m/e=258 (M+).

후처리

  1. filtrationthe formed precipitate is filtered off
  2. washWashing with methanol

출처 및 근거

ORD 기록
ord-5839654b6f0142cb9858bb4545e168df
출처 데이터셋
uspto-grants-2008_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07317007B2

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