HCID 59643063, 화합물 → HCID 59643052, 화합물

HRID 2251612노트

반응식

HRID 2251612 반응식
[C:1]([C:4]1[CH:9]=[CH:8][C:7]([O:10][CH2:11][O:12][CH3:13])=[C:6]([O:14][CH3:15])[CH:5]=1)([CH3:3])=[CH2:2]>CO.[Pd]>[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([O:10][CH2:11][O:12][CH3:13])=[C:6]([O:14][CH3:15])[CH:5]=1)([CH3:3])[CH3:2]

참가 물질

4

반응물 1

HCID 59643063HCID 59643063, 화합물

생성물 1

HCID 59643052HCID 59643052, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

To a solution of 4-isopropenyl-2-methoxy-1-methoxymethoxy-benzene (3.5 g, 16.81 mmol) in 20 mL MeOH, Pd/C (10%, 350 mg) was added and the mixture was stirred 16 h under a H2 atmosphere. The reaction mixture was then filtered through Celite and evaporated in vacuo and briefly dried under vacuum to yield the title compound as a colorless oil.

후처리

  1. filtrationThe reaction mixture was then filtered through Celite
  2. customevaporated in vacuo
  3. custombriefly dried under vacuum

출처 및 근거

ORD 기록
ord-9268edd1e713488bb67119630f1e5147
출처 데이터셋
uspto-grants-2008_01
특허 번호
US07319101B2

반응 노트

불러오는 중…