3,4-Difluorobenzeneboronic acid → HCID 69040293, 화합물

반응식

[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][CH:7]=[C:8](OS(C(F)(F)F)(=O)=O)[CH:9]=2)[C:4](=[O:19])[CH2:3]1.[F:21][C:22]1[CH:23]=[C:24](B(O)O)[CH:25]=[CH:26][C:27]=1[F:28]>>[F:21][C:22]1[CH:23]=[C:24]([C:8]2[CH:9]=[C:10]3[C:5](=[CH:6][CH:7]=2)[C:4](=[O:19])[CH2:3][C:2]3([CH3:1])[CH3:20])[CH:25]=[CH:26][C:27]=1[F:28]

참가 물질

반응물 2

HCID 27343373,4-Difluorobenzeneboronic acid

HCID 57618520Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester

생성물 1

HCID 69040293HCID 69040293, 화합물

실험 절차

The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 3,4-difluorophenyl boronic acid according to the procedure described in example 21. MS m/z 273; HRMS: calcd for C17H14F2O+H+, 273.10855; found (ESI, [M+H]+), 273.1078.

출처 및 근거

ORD 기록: ord-2dcb6e014df745799c77f80a786309e4
출처 데이터셋: uspto-grants-2008_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07319152B2

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