Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Chloro-2-methylaniline → N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Chloro-2-methylaniline | HCID 6894 | — |
| 반응물 | 4-Chlorobenzaldehyde | HCID 7726 | — |
| 생성물 | N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline | HCID 13017553 | — |
반응 단계
2-methyl-3-chloroaniline (0.25 mole) and 4-chlorobenzaldehyde (0.25 mole) were ground in a mortar. The mixture was heated, with stirring in a water bath for 1.5 hours. Distillation at reduced pressure gave N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline as a second fraction; B.p. 139° C./0.020 mm.; m.p. 79°-81° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04235929 |
| 출처 데이터셋 | uspto-grants-1980_11 |
| ORD ID | ord-f9d5df113c0a460b9c19606b5d3fecad |
| 출처 메모 | uspto-grants-1980_11 |