참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethyl maleate | HCID 5271565 | — |
| 반응물 | Dimethylphosphite | HCID 21884954 | — |
| 용매 | Sodium Methoxide | HCID 10942334 | — |
| 생성물 | Dimethyl (dimethoxyphosphinyl)succinate | HCID 102330 | — |
반응 단계
20 ml of 5% sodium methylate solution are added dropwise to 144 g (1 mol) of dimethyl maleate and 110 g of dimethyl phosphite until the exothermic reaction is completed. The reaction mixture is stirred for a further 30 minutes at 100° C. and then freed from low volatility constituents.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04235976 |
|---|
| 출처 데이터셋 | uspto-grants-1980_11 |
|---|
| ORD ID | ord-a86589083614466a91c3fab371711d9b |
|---|
| 출처 메모 | uspto-grants-1980_11 |
|---|
