Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium periodate → Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium periodate | HCID 516896 | — |
| 반응물 | 1,4-Dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol | HCID 23329608 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehyde | HCID 88785356 | — |
반응 단계
One gram of 1,4-dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol, is suspended in 30 ml. of an aqueous solution containing 0.77 g. of potassium periodate and one ml. of ethanol. After stirring at room temperature for 24 hours the insoluble material is removed by filtration, washed well with water and dried leaving a yellow product, m.p. 129°-132° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04235996 |
| 출처 데이터셋 | uspto-grants-1980_11 |
| ORD ID | ord-cb2cb3b108aa4d2da3ce5f436af99830 |
| 출처 메모 | uspto-grants-1980_11 |