Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenolphthalein → (-)-alpha-Amino-4-hydroxy-3-(methoxymethyl)benzeneacetic acid methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenolphthalein | HCID 4764 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | (-)-alpha-Amino-4-hydroxy-3-(methoxymethyl)benzeneacetic acid methyl ester hydrochloride | HCID 70585116 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (-)-alpha-Amino-4-hydroxy-3-(methoxymethyl)benzeneacetic acid methyl ester | HCID 53644499 | — |
반응 단계
(-)-α-Amino-4-hydroxy-3-(methoxymethyl)benzeneacetic acid methyl ester hydrochloride is dissolved in a minimum amount of methanol. To this solution is added methanolic potassium hydroxide until a basic reaction to phenolphthalein is observed. The potassium chloride which precipitates is removed and the solvent is removed under vacuum to give a quantitative yield of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04236002 |
| 출처 데이터셋 | uspto-grants-1980_11 |
| ORD ID | ord-22c0988786fe4376a47651056bc6e2c5 |
| 출처 메모 | uspto-grants-1980_11 |