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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2253460생성일: 2026년 10월 27일

2-Chlorobenzenesulfonamide → 2-chloro-N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamide

https://huagongshe.com/reaction/2253460

반응식

참여 물질

역할이름HCID투입량
반응물2-ChlorobenzenesulfonamideHCID 81410—
반응물3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acidHCID 3036152—
생성물2-chloro-N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamideHCID 69316648—

반응 단계

Prepared by coupling 1a and 2-chlorobenzenesulfonamide in accordance with Procedure 1, Method B described hereinabove. Yield (19%); 1H NMR (d6-DMSO) δ 12.56 (s, 1H), 8.09 (d, J=7.7 Hz, 1H), 7.69-7.53 (m, 3H), 7.39-7.08 (m, 13H), 6.85 (d, J=8.1 Hz, 2H), 6.47 (d, J=15.8 Hz, 1H), 2.36 (q, J=7.3 Hz, 2H), 0.82 (t, J=7.3 Hz, 3H); APcI m/z: 528 (M+H+).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07323587B2
출처 데이터셋uspto-grants-2008_01
ORD IDord-e6466392f2a641dfbfc41d33fda28fb2
출처 메모uspto-grants-2008_01