Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → Methyl 3-(chlorocarbonyl)-5-nitrobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 1,3-Benzenedicarboxylic acid, 5-nitro-, 1-methyl ester | HCID 74776 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Methyl 3-(chlorocarbonyl)-5-nitrobenzoate | HCID 74774 | — |
반응 단계
Heat 3-methoxycarbonyl-5-nitrobenzoic acid (2.0 g=8.9 mmol) with SOCl2 (2.1 g=18 mmol) in toluene at reflux 1 hr. Concentrate to obtain 3-methoxycarbonyl-5-nitrobenzoyl chloride, m.p. 66°-8° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05232920 |
| 출처 데이터셋 | uspto-grants-1993_08 |
| ORD ID | ord-58d1af3e19f64ebeaafb93c0ff9d8920 |
| 출처 메모 | uspto-grants-1993_08 |