Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Phenacyltetrahydrothiophenium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Tetrahydrothiophene | HCID 1127 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Phenacyl bromide | HCID 6259 | — |
| 용매 | Nitromethane | HCID 6375 | — |
| 생성물 | Phenacyltetrahydrothiophenium bromide | HCID 11346720 | — |
반응 단계
88.2 g (0.44 mole) of phenacyl bromide and 39.1 g (0.44 mole) of tetrahydrothiophene were dissolved in 220 g of nitromethane, which was stirred for 4 hours at room temperature. 800 g of water and 400 g of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, phenacyltetrahydrothiophenium bromide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07556909B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-e340a01c97f3477caf8d844c91753b25 |
| 출처 메모 | uspto-grants-2009_07 |