4-Iodoaniline → N-(4-iodophenyl)-N-methylethanesulphonamide

HRID 2254666

반응식

[I:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.I[C:10]1C=CC(NS(C)(=O)=O)=CC=1.[CH2:21]([S:23](Cl)(=[O:25])=[O:24])[CH3:22]>>[I:1][C:2]1[CH:8]=[CH:7][C:5]([N:6]([CH3:10])[S:23]([CH2:21][CH3:22])(=[O:25])=[O:24])=[CH:4][CH:3]=1

참가 물질

반응물 3

HCID 108934-Iodoaniline

HCID 11667Ethanesulfonyl chloride

HCID 836147N-(4-iodophenyl)methanesulfonamide

생성물 1

HCID 19785600N-(4-iodophenyl)-N-methylethanesulphonamide

실험 절차

The product so obtained was used in place of 4-iodoaniline in the procedure described in Example 3 for the preparation of N-(4-iodophenyl)methanesulphonamide and ethanesulphonyl chloride was used in place of methanesulphonyl chloride. Thus was obtained N-(4-iodophenyl)-N-methylethanesulphonamide as an oil.

후처리

customThe product so obtained

출처 및 근거

ORD 기록: ord-91afd57f1359434bbea2679366060af5
출처 데이터셋: uspto-grants-1993_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05236948

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