Dimethylamine → 5-Nitro-6-dimethylaminoquinoline

HRID 2257186

반응식

HRID 2257186 반응식
[N+:1]([C:4]1[C:13](Cl)=[CH:12][CH:11]=[C:10]2[C:5]=1[CH:6]=[CH:7][CH:8]=[N:9]2)([O-:3])=[O:2].[CH3:15][NH:16][CH3:17]>>[N+:1]([C:4]1[C:13]([N:16]([CH3:17])[CH3:15])=[CH:12][CH:11]=[C:10]2[C:5]=1[CH:6]=[CH:7][CH:8]=[N:9]2)([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 674DimethylamineHCID 40708006-Chloro-5-nitroquinoline

생성물 1

HCID 190278695-Nitro-6-dimethylaminoquinoline

실험 절차

5-Nitro-6-chloroquinoline, prepared as described by Manske & Kulka, Organic Reactions, Vol. VII, 59 (1953) and Campbell et al., J. Am. Chem. Soc., 68, 1559 (1946), was allowed to react with dimethylamine to yield 5-nitro-6-dimethylaminoquinoline. This material was converted to the title compound by the procedure described in Example 33.

출처 및 근거

ORD 기록
ord-aaeee53c8bd74854b4c49490fa0f8acd
출처 데이터셋
uspto-grants-1997_08
특허 번호
US05656634

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