참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 3-Chloro-2-methyl-1-propene | HCID 11241 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | N-Butylaniline | HCID 14310 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-butyl-N-(2-methylprop-2-eneyl)aniline | HCID 54010992 | — |
반응 단계
A mixture of N-butylaniline (12.35 parts), anhydrous potassium carbonate (17.1 parts), 3-chloro-2-methylpropene (11.24 parts) and DMF (20 parts) was stirred at 90° C. for 8 hours. The cooled mixture was poured into toluene, washed with water (×2), 1N hydrochloric acid (30 parts) and water (×2). The dried organic phase was evaporated to leave N-butyl-N-(2-methylprop-2-eneyl)aniline (14.3 parts).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05660598 |
|---|
| 출처 데이터셋 | uspto-grants-1997_08 |
|---|
| ORD ID | ord-fbce872db8c94b7daf813f5029f98905 |
|---|
| 출처 메모 | uspto-grants-1997_08 |
|---|
