Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
O-Xylene → 1-Butyl-2,2-dimethylindoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | O-Xylene | HCID 7237 | — |
| 반응물 | N-butyl-N-(2-methylprop-2-eneyl)aniline | HCID 54010992 | — |
| 촉매 | Zincchloride | HCID 3007855 | — |
| 생성물 | 1-Butyl-2,2-dimethylindoline | HCID 18788042 | — |
반응 단계
A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05660598 |
| 출처 데이터셋 | uspto-grants-1997_08 |
| ORD ID | ord-7f603290ea884b37aa05920e12f26970 |
| 출처 메모 | uspto-grants-1997_08 |