Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methylindole-2-carboxaldehyde → 3,4-Dimethyl-2-(methylaminomethyl)thieno[2,3-b]thiophene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methylindole-2-carboxaldehyde | HCID 267164 | — |
| 반응물 | 3,4-Dimethylthieno[2,3-B]Thiophene-2-Carbaldehyde | HCID 2778771 | — |
| 생성물 | 3,4-Dimethyl-2-(methylaminomethyl)thieno[2,3-b]thiophene | HCID 22593756 | 53% |
반응 단계
According to the procedure of Preparation 24(a), except substituting 3,4-dimethylthieno[2,3-b]thiophene-2-carboxaldehyde (0.5 g, 2.5 mmole) for the 1-methylindole-2-carboxaldehyde, the title compound (0.28 g, 53%) was prepared as a colorless oil: MS (ES) m/e 212 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07557125B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-2ed4e6cc15e7466c85d7d1c0f3c77dbb |
| 출처 메모 | uspto-grants-2009_07 |