Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isophthalaldehyde → 3-(2-(7-Chloroquinolin-2-yl)vinyl)benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isophthalaldehyde | HCID 34777 | — |
| 반응물 | 7-Chloro-2-methylquinoline | HCID 138395 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 용매 | Acetic Anhydride | HCID 7918 | — |
| 생성물 | 3-(2-(7-Chloroquinolin-2-yl)vinyl)benzaldehyde | HCID 53394853 | — |
반응 단계
A solution of isophthalaldehyde (4.0 g) and 7-chloroquinaldine (5.39 g) in acetic anhydride was heated at 125° in an oil bath for 48 hours. The reaction was cooled to room temperature, diluted with ether (30 mL) and the resulting suspension was stirred vigorously. The solid title compound was collected by filtration and was used as such in the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05428171 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-82aa24b70650476f8934154e035255ed |
| 출처 메모 | uspto-grants-1995_06 |