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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2260110생성일: 2026년 10월 26일

1H-Indazole-5,6-diamine → 6-(5-chlorothien-2-yl)-1H-pyrazolo[3,4-g]quinoxaline 7-(5-chlorothien-2-yl)-1H-pyrazolo[3,4-g]quinoxaline

https://huagongshe.com/reaction/2260110

반응식

참여 물질

역할이름HCID투입량
반응물1H-Indazole-5,6-diamineHCID 81900—
반응물2-Chloro-5-glyoxyloylthiopheneHCID 18788710—
용매EthanolHCID 702—
생성물6-(5-chlorothien-2-yl)-1H-pyrazolo[3,4-g]quinoxaline 7-(5-chlorothien-2-yl)-1H-pyrazolo[3,4-g]quinoxalineHCID 18999820—

반응 단계

To a mixture of 5,6-diaminoindazole (0.5 g) in 30 ml absolute ethanol is added slowly a solution of 2-chloro-5-glyoxyloylthiophene (0.72 g) and 20 ml ethanol. The resulting mixture is stirred at room temperature for 4.5 hours. The yellow solid which forms is filtered off, washed with ethanol then with hexane and air dried overnight.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05476851
출처 데이터셋uspto-grants-1995_12
ORD IDord-5922bbc9349b42c8bc5ca660f6846243
출처 메모uspto-grants-1995_12