Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3,7,11,15-Tetramethylhexadecanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Phytanic Acid | HCID 26840 | — |
| 촉매 | Pyridine | HCID 1049 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 3,7,11,15-Tetramethylhexadecanoyl chloride | HCID 14802143 | 98.2% |
반응 단계
Under a nitrogen atmosphere, one drop of pyridine was added to 2.5 g of phytanic acid and 12.5 ml of methylene chloride, and 1.43 g of thionyl chloride was added dropwise thereto at room temperature. After the completion of dropwise addition, the resultant was refluxed for 1 hour, and concentrated under reduced pressure to obtain about 2.6 g of phytanic acid chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07846903B2 |
| 출처 데이터셋 | uspto-grants-2010_12 |
| ORD ID | ord-856cd64f0a5f413198dbd4061f6bead4 |
| 출처 메모 | uspto-grants-2010_12 |