Thionyl Chloride → HCID 14674299, 화합물
반응식
[C:1]([C:5]1[CH:9]=[C:8]([CH2:10]O)[O:7][N:6]=1)([CH3:4])([CH3:3])[CH3:2].S(Cl)([Cl:14])=O>ClCCl>[C:1]([C:5]1[CH:9]=[C:8]([CH2:10][Cl:14])[O:7][N:6]=1)([CH3:4])([CH3:3])[CH3:2]참가 물질
4
실험 절차
1.12 g of (3-t-butyl-isoxazol-5-yl)methanol was dissolved in 35 ml of dichloromethane, and 2.4 ml of thionyl chloride was added. The mixture was stirred at room temperature overnight. The reaction mixture was concentrated under reduced pressure. The residue was washed with hexane to obtain 1.12 g of 3-t-butyl-5-(chloromethyl)-isoxazole.
후처리
- concentrationThe reaction mixture was concentrated under reduced pressure
- washThe residue was washed with hexane
출처 및 근거
- ORD 기록
- ord-356e4e5682644567a3388782d38711a5
- 출처 데이터셋
- uspto-grants-2010_12
- 특허 번호
- US07846956B2
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