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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2262349생성일: 2026년 10월 25일

4-nitro-N-(2-diethylamino-ethyl)-2-methoxy-benzamide → 4-Amino-N-[2-(diethylamino)ethyl]-2-methoxybenzamide

https://huagongshe.com/reaction/2262349

반응식

참여 물질

역할이름HCID투입량
반응물4-nitro-N-(2-diethylamino-ethyl)-2-methoxy-benzamideHCID 408891—
촉매PalladiumHCID 23938—
용매Tetrahydrofuran ethanolHCID 21873804—
생성물4-Amino-N-[2-(diethylamino)ethyl]-2-methoxybenzamideHCID 77374106.4%

반응 단계

5.7 g (19.3 mmol) of 4-nitro-N-(2-diethylamino-ethyl)-2-methoxy-benzamide is dissolved in 120 ml of tetrahydrofuran:ethanol 1:1>mixed with 2 g of palladium on carbon (10%×50% water) and hydrogenated for 1 hour at room temperature and normal pressure. After being drawn off on diatomaceous earth and after concentration by evaporation, 5.45 g of 4-amino-N-(2-diethylamino-ethyl)-2-methoxy-benzamide is obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07850948B2
출처 데이터셋uspto-grants-2010_12
ORD IDord-fec49c96a0654ddaa3d16ec6f4872d02
출처 메모uspto-grants-2010_12