4-Methylpyridine → 1-(4-Acetoxybutyl)-4-methyl-pyridinium iodide

HRID 2264860노트

반응식

HRID 2264860 반응식
[N:1]1[CH:6]=[CH:5][C:4]([CH3:7])=[CH:3][CH:2]=1.[I:8][CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14](=[O:16])[CH3:15]>CCOCC>[I-:8].[C:14]([O:13][CH2:12][CH2:11][CH2:10][CH2:9][N+:1]1[CH:6]=[CH:5][C:4]([CH3:7])=[CH:3][CH:2]=1)(=[O:16])[CH3:15]

참가 물질

4

반응물 2

HCID 79634-MethylpyridineHCID 27334054-Iodobutyl acetate

생성물 1

HCID 687814631-(4-Acetoxybutyl)-4-methyl-pyridinium iodide

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

10 mmol (0.93 g) γ-picoline and 10 mmol (2.42 g) 4-iodobutylacetate are heated 4 h at 120° C. and after cooling repeatedly stirred with ether, decanted a finally dried in vacuum.

후처리

  1. temperatureafter cooling repeatedly
  2. customdecanted
  3. customa finally dried in vacuum

출처 및 근거

ORD 기록
ord-a7c4bc6d527b4e8d97a03b4f193d3b19
출처 데이터셋
uspto-grants-2010_12
특허 번호
US07855293B2

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