Butanethioic acid, 3-oxo-, S-(1,1-dimethylethyl) ester → 2-(2-chloro-4-methanesulfonylbenzyl)-3-oxothiobutyric acid S-tert-butyl Ester

HRID 2266522노트

반응식

HRID 2266522 반응식
Br[CH2:2][C:3]1[CH:8]=[CH:7][C:6]([S:9]([CH3:12])(=[O:11])=[O:10])=[CH:5][C:4]=1[Cl:13].[C:14]([S:18][C:19](=[O:24])[CH2:20][C:21](=[O:23])[CH3:22])([CH3:17])([CH3:16])[CH3:15]>>[C:14]([S:18][C:19](=[O:24])[CH:20]([CH2:2][C:3]1[CH:8]=[CH:7][C:6]([S:9]([CH3:12])(=[O:11])=[O:10])=[CH:5][C:4]=1[Cl:13])[C:21](=[O:23])[CH3:22])([CH3:17])([CH3:15])[CH3:16]

참가 물질

3

반응물 2

HCID 140007Butanethioic acid, 3-oxo-, S-(1,1-dimethylethyl) esterHCID 27610831-(Bromomethyl)-2-chloro-4-(methylsulfonyl)benzene

생성물 1

HCID 866314412-(2-chloro-4-methanesulfonylbenzyl)-3-oxothiobutyric acid S-tert-butyl Ester

실험 절차

The title compound was prepared by the method of Preparation 34a using 1-bromomethyl-2-chloro-4-methanesulfonylbenzene and 3-oxothiobutyric acid S-tert-butyl ester.

출처 및 근거

ORD 기록
ord-ac175087c6b44dc3a50614a8f539538e
출처 데이터셋
uspto-grants-2010_12
특허 번호
US07858640B2

반응 노트

불러오는 중…