3-Chloro-4-methoxybenzylamine → HCID 10338602, 화합물

반응식

C([O:3][C:4]([C:6]1[C:7](Cl)=[C:8]2[CH:14]=[N:13][N:12]([CH2:15][CH3:16])[C:9]2=[N:10][CH:11]=1)=[O:5])C.[Cl:18][C:19]1[CH:20]=[C:21]([CH2:27][NH2:28])[CH:22]=[CH:23][C:24]=1[O:25][CH3:26]>>[Cl:18][C:19]1[CH:20]=[C:21]([CH2:27][NH:28][C:7]2[C:6]([C:4]([OH:3])=[O:5])=[CH:11][N:10]=[C:9]3[N:12]([CH2:15][CH3:16])[N:13]=[CH:14][C:8]=23)[CH:22]=[CH:23][C:24]=1[O:25][CH3:26]

참가 물질

반응물 2

HCID 7380383-Chloro-4-methoxybenzylamine

HCID 10491120ethyl 4-chloro-1-ethyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylate

생성물 1

HCID 10338602HCID 10338602, 화합물수율 87%

실험 절차

4-Chloro-1-ethyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid ethyl ester and (3-chloro-4-methoxyphenyl)methylamine was used to afford the title compound (87%) as a white solid: mp 250 ° C.(decomposed).

출처 및 근거

ORD 기록: ord-206d03dd839348ce908c28f9f1c70708
출처 데이터셋: uspto-grants-2001_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06326379B1

반응 노트

불러오는 중…