3,3'-Dithiodipropionic acid → Disodium 3,3'-dithiobispropionate

HRID 2269537노트

반응식

HRID 2269537 반응식
C(=O)([O-])O.[Na+:5].[C:6]([OH:17])(=[O:16])[CH2:7][CH2:8][S:9][S:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14]>O>[C:6]([O-:17])(=[O:16])[CH2:7][CH2:8][S:9][S:10][CH2:11][CH2:12][C:13]([O-:15])=[O:14].[Na+:5].[Na+:5]

참가 물질

5

반응물 3

HCID 951163,3'-Dithiodipropionic acidHCID 516892Sodium BicarbonateHCID 178435178HCID 178435178, 화합물

생성물 1

HCID 6454427Disodium 3,3'-dithiobispropionate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A 1-liter polypropylene beaker was charged with a solution of 42 g (0.50 mole) of sodium hydrogen carbonate in 100 g of distilled water, followed by the slow addition of 52.5 g (0.25 mole) of 3,3′-dithiodipropionic acid, which required about 10 minutes. The resulting paste was spread on an evaporating tray and dried. The salt product was white-colored and melted above 225° C.

후처리

  1. customdried
  2. custommelted above 225° C.

출처 및 근거

ORD 기록
ord-c0b0802a4a274e109a330d1de8d25fb9
출처 데이터셋
uspto-grants-2001_12
특허 번호
US06329455B1

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