Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Fluoroaniline → HCID 178500755, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Fluoroaniline | HCID 9742 | — |
| 반응물 | 2-(3,4-Dimethyl-benzoyl)-3-methoxy-acrylic acid methyl ester | HCID 66879272 | — |
| 반응물 | HCID 178500760 | HCID 178500760 | — |
| 생성물 | HCID 178500755 | HCID 178500755 | 50.1% |
반응 단계
Compound 2h was prepared following the procedure described in Step 1 of Example 1 using from 2g (8.06 mmol) of crude 2-(3,4-Dimethyl-benzoyl)-3-methoxy-acrylic acid methyl ester 1a and 0.806 g (7.26 mmol) 3-fluoroaniline. The crude product 2h was purified by recrystalization with dichloromethane/hexane to yield 1.19 g of 2-(3,4-Dimethyl-benzoyl)-3-(3-fluoro-phenylamino)-acrylic acid methyl ester as a brown solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07557213B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-19c6e3c0780148ec87451d8ba239704c |
| 출처 메모 | uspto-grants-2009_07 |