Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenol, 4-methoxy-2-nitro- → 2-Amino-4-methoxyphenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenol, 4-methoxy-2-nitro- | HCID 15285 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-Amino-4-methoxyphenol | HCID 1419108 | — |
반응 단계
A solution of 4-methoxy-2-nitrophenol 11 (10 g, 59.1 mmol) and Pd/C (1.0 g) in methanol (100 ml) was placed on a Parr shaker under H2 (50 psi) for 60 minutes. The reaction mixture was filtered through Celite 521 and the filter cake washed with MeOH. The filtrate was evaporated (in vacuo), to yield compound 12 as a tan solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849632B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-4d5d8283e50c4141aca07510c1511933 |
| 출처 메모 | uspto-grants-2005_02 |