Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenol, 4-methoxy-2-nitro- → 2-Amino-4-methoxyphenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenol, 4-methoxy-2-nitro- | HCID 15285 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-Amino-4-methoxyphenol | HCID 1419108 | — |
반응 단계
Commercially available 4-methoxy-2-nitrophenol (1 g, 5.9 mmol), a compound of formula (C) was dissolved in 10 mL of methanol, and then 10% Pd/C was added to the mixture. The mixture was hydrogenated in a Parr™ shaker at 30 psi until consumption of hydrogen stopped. The mixture was filtered through Celite and concentrated, to yield 2-amino-4-methoxyphenol a compound of formula (d), which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849632B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-357d0f6dda4445b290f863c893983868 |
| 출처 메모 | uspto-grants-2005_02 |