HCID 75480723, 화합물 → 5-(Pyrrolidin-1-yl)pyridin-2-amine
반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH2:14][CH2:13][CH2:12][CH2:11]2)=[CH:6][N:5]=1)([O-])=O>[Pd]>[N:10]1([C:7]2[CH:8]=[CH:9][C:4]([NH2:1])=[N:5][CH:6]=2)[CH2:14][CH2:13][CH2:12][CH2:11]1참가 물질
3
실험 절차
410 mg (2.12 mmol) of the product obtained in step 25.1 are hydrogenated in the presence of 10% Pd/C at atmospheric pressure at 35° C. The solution obtained is evaporated under reduced pressure to give 321 mg of 5-pyrrolidin-1-ylpyridin-2-ylamine.
후처리
- customThe solution obtained
- customis evaporated under reduced pressure
출처 및 근거
- ORD 기록
- ord-8d3f3af05ba7426988771a7bdc2ec61c
- 출처 데이터셋
- uspto-grants-2015_09
- 특허 번호
- US09120812B2
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