Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorotrimethylsilane → N,N-bis(trimethylsilyl)perfluorooctaneamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | Hexadecane | HCID 11006 | — |
| 반응물 | 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctanamide | HCID 67919 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | N,N-bis(trimethylsilyl)perfluorooctaneamide | HCID 86615112 | — |
반응 단계
First, perfluorooctaneamide (CF3(CF2)7CONH2) (46 g) was dissolved in n-hexane (300 ml). Thereafter, trimethylchlorosilane (15 ml) was dropped gradually into the solution obtained above, in a dry nitrogen atmosphere. Then this was allowed to react for two hours while being stirred. After the reaction was completed, hexadecane contained in the reaction solution was removed with the evaporator. Thus, N,N-bis(trimethylsilyl)perfluorooctaneamide was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07560301B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-297020bd8b424536ad1a50bc562a8510 |
| 출처 메모 | uspto-grants-2009_07 |