Triethylamine → HCID 22273083, 화합물

HRID 227375

반응식

HRID 227375 반응식
[O:1]1[CH2:6][CH2:5][CH:4]([CH2:7][CH2:8][OH:9])[CH2:3][CH2:2]1.C(N(CC)CC)C.[CH3:17][S:18](Cl)(=[O:20])=[O:19]>O1CCCC1>[CH3:17][S:18]([O:9][CH2:8][CH2:7][CH:4]1[CH2:5][CH2:6][O:1][CH2:2][CH2:3]1)(=[O:20])=[O:19]

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 177509442-(Oxan-4-yl)ethan-1-ol

생성물 1

HCID 22273083HCID 22273083, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The product of Example 8A (2.9 mmol), triethylamine (1.2 mL, 8.7 mmol) and methanesulfonyl chloride (0.34 mL, 4.4 mmol) in 10 mL tetrahydrofuran (THF) were reacted and the product isolated as in Example 1C to give the title compound that was used directly in the next reaction.

후처리

  1. customthe product isolated as in Example 1C

출처 및 근거

ORD 기록
ord-cab984eb0dbd4e83a9687a4e09548263
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07560481B2

연결된 노트

불러오는 중…