2-Methoxyethanol → 2-Methoxyethyl methanesulfonate

HRID 227378

반응식

HRID 227378 반응식
[CH3:1][O:2][CH2:3][CH2:4][OH:5].C(N(CC)CC)C.[CH3:13][S:14](Cl)(=[O:16])=[O:15]>C1COCC1>[CH3:13][S:14]([O:5][CH2:4][CH2:3][O:2][CH3:1])(=[O:16])=[O:15]

참가 물질

5

반응물 3

HCID 80192-MethoxyethanolHCID 8471TriethylamineHCID 31297Methanesulfonyl chloride

생성물 1

HCID 1462932-Methoxyethyl methanesulfonate

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The 2-methoxyethanol (Aldrich, 94 mg, 1.2 mmol), triethylamine (0.56 mL, 4.1 mmol), and methanesulfonyl chloride (0.15 mL, 1.9 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.

출처 및 근거

ORD 기록
ord-87dadd40ed0c406289cd56a7199a6f88
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07560481B2

연결된 노트

불러오는 중…