Triethylamine → HCID 13077377, 화합물

HRID 227387노트

반응식

HRID 227387 반응식
[OH:1][CH2:2][CH2:3][N:4]1[CH:8]=[CH:7][CH:6]=[CH:5]1.C(N(CC)CC)C.[CH3:16][S:17](Cl)(=[O:19])=[O:18]>C1COCC1>[CH3:16][S:17]([O:1][CH2:2][CH2:3][N:4]1[CH:8]=[CH:7][CH:6]=[CH:5]1)(=[O:19])=[O:18]

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 109754381-(2-Hydroxyethyl)pyrrole

생성물 1

HCID 13077377HCID 13077377, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The 1-(2-hydroxyethyl)pyrrole (TCI-US, 0.138 g, 1.2 mmol), triethylamine (0.56 mL, 4.1 mmol), and methanesulfonyl chloride (0.15 mL, 1.9 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.

출처 및 근거

ORD 기록
ord-613ac5b4ba6340f09a7201912487446c
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07560481B2

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