Triethylamine → HCID 13709828, 화합물

HRID 227400

반응식

HRID 227400 반응식
[CH2:1]([O:8][CH2:9][CH2:10][CH2:11][OH:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(N(CC)CC)C.[CH3:20][S:21](Cl)(=[O:23])=[O:22]>C1COCC1>[CH3:20][S:21]([O:12][CH2:11][CH2:10][CH2:9][O:8][CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)(=[O:23])=[O:22]

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 3479713-Benzyloxy-1-propanol

생성물 1

HCID 13709828HCID 13709828, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The 3-benzyloxypropanol (Aldrich, 0.28 g, 1.7 mmol), triethylamine (0.67 mL, 5.0 mmol), and methanesulfonyl chloride (0.19 mL, 2.5 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.

출처 및 근거

ORD 기록
ord-14a41b641afb4048929263df096dff8f
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07560481B2

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