Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1,3,3-Tetramethylbutyl isocyanide → [6,8-Dibromo-2-(2,3-dimethoxyphenyl)-5-methylimidazo[1,2-a]pyridin-3-yl]-(1,1,3,3-tetramethylbutyl)-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| 반응물 | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| 반응물 | Wisteria sinensis, ext. | HCID 522994 | — |
| 용매 | Perchloric Acid | HCID 24247 | — |
| 생성물 | [6,8-Dibromo-2-(2,3-dimethoxyphenyl)-5-methylimidazo[1,2-a]pyridin-3-yl]-(1,1,3,3-tetramethylbutyl)-amine | HCID 9829072 | — |
반응 단계
Compound (6) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3,5-dibromo-6-methylpyridine solution (0.1 M, DCM), 0.575 ml of 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, DCM), 0.500 ml of 2,3-dimethoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849642B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-2162421c093a43f59d81760000eb9656 |
| 출처 메모 | uspto-grants-2005_02 |